Spectroscopie FTIR

Equipment allowing the analysis of the vibration modes of molecules in the middle infrared (4000 - 400 cm^-1) in transmission and attenuated total reflectance (ATR mode with a diamond crystal). The analysis of liquid samples is possible thanks to a specific cell in transmission but also in ATR mode (Ge crystal). The coupling of this spectrometer with our thermogravimetric analyzer (ATG) will allow to follow the gaseous products resulting from the thermal decomposition of various samples by adding a heated gas cell and a heated transfer line that link the two equipments.

FTIR spectrometer	Model Nicolet iS50 Thermo Scientific
Technical specifications	Types of samples : solid, liquid, gas samples (coupling with TGA)
	- Measurement in the IR medium : 4000 - 400 cm-1 – Source MIR Polaris – Dynamic alignment Michelson interferometer – Separator KBr with Germanium coating – Detector: DLaTGS with window in KBr – Integrated ATR module with diamond crystal – 2 liquid exchange cells: specific cell for transmission, specific cell for ATR mode with Ge crystal - Possible coupling with TGA for the analysis of gaseous thermal decomposition products
Persons in charge of the tool Associated team	Scientific manager : – Alejandro Fernandez-Martinez 04 76 63 51 97 Technical manager : – Valérie Magnin 04 76 51 40 78